Publication:
Crystal structure of 4-methoxy-N-(piperidine-1carbonothioyl)benzamide

Simple item page
dc.contributor.authorSuhud, Ken_US
dc.contributor.authorHasbullah, SAen_US
dc.contributor.authorAhmad, Men_US
dc.contributor.authorHeng, LYen_US
dc.contributor.authorKassim, MBen_US
dc.date.accessioned2024-05-29T02:51:47Z
dc.date.available2024-05-29T02:51:47Z
dc.date.issued2017
dc.description.abstractIn the title compound, C14H18N2O2S, the piperidine ring has a chair conformation. Its mean plane is twisted with respect to the 4-methoxybenzoyl ring, with a dihedral angle of 63.0 (3)degrees. The central N-C(=S)-N(H)-C(=O) bridge is twisted with an N-C-N-C torsion angle of 74.8 (6)degrees. In the crystal, molecules are linked by N-H center dot center dot center dot O and C-H center dot center dot center dot O hydrogen bonds, forming chains along the c-axis direction. Adjacent chains are linked by C-H center dot center dot center dot pi interactions, forming layers parallel to the ac plane. The layers are linked by offset pi-pi interactions [intercentroid distance = 3.927 (3) angstrom], forming a supramolecular three-dimensional structure.
dc.identifier.doi10.1107/S2056989017013317
dc.identifier.epage+
dc.identifier.issn2056-9890
dc.identifier.scopusWOS:000412026700030
dc.identifier.spage1530
dc.identifier.urihttps://oarep.usim.edu.my/handle/123456789/11239
dc.identifier.volume73
dc.languageEnglish
dc.language.isoen_USen_US
dc.publisherInt Union Crystallographyen_US
dc.relation.ispartofActa Crystallographica Section E-Crystallographic Communications
dc.sourceWeb Of Science (ISI)
dc.subjectcrystal structureen_US
dc.subjectbenzoylthioureaen_US
dc.subjectpiperidineen_US
dc.subjectpyrrolidineen_US
dc.subjectbenzamideen_US
dc.subjectanti-cancer hydrogen bondingen_US
dc.subjectC-H center dot center dot center dot pi interactionsen_US
dc.subjectoffset pi-pi interactionsen_US
dc.titleCrystal structure of 4-methoxy-N-(piperidine-1carbonothioyl)benzamideen_US
dc.typeArticleen_US
dspace.entity.typePublication

Files

Original bundle
Now showing 1 - 1 of 1
Thumbnail Image
Name:
Crystal structure of 4-methoxy-N-[(pyrrolidin-1-yl)carbothioyl]benzamide.pdf
Size:
357.22 KB
Format:
Adobe Portable Document Format
Download

Collections

Web of Science_WoS